Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals

A. Shavel, M. Ibáñez, Z. Luo, J. De Roo, A. Carrete, M. Dimitrievska, A. Genç, M. Meyns, A. Pérez Rodríguez, M. Kovalenko, J. Arbol, A. Cabot, Chemistry of Materials 28 (2016) 720–726.

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Journal Article | Published | English
Author
Shavel, Alexey; Ibanez Sabate, MariaIST Austria ; Luo, Zhishan; De Roo, Jonathan; Carrete, Alex; Dimitrievska, Mirjana; Genç, Aziz; Meyns, Michaela; Pérez Rodríguez, Alejandro; Kovalenko, Maksym; Arbol, Jordi; Cabot, Andreu
All
Abstract
Monodisperse Cu2ZnSnS4 (CZTS) nanocrystals (NCs), with quasi-spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. Optimized synthetic conditions allowed the production of several grams of highly monodisperse CZTS NCs per batch, with up to 5 wt % concentration in a crude solution and a yield above 90%.
Publishing Year
Date Published
2016-01-17
Journal Title
Chemistry of Materials
Volume
28
Issue
3
Page
720 - 726
IST-REx-ID
379

Cite this

Shavel A, Ibáñez M, Luo Z, et al. Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals. Chemistry of Materials. 2016;28(3):720-726. doi:10.1021/acs.chemmater.5b03417
Shavel, A., Ibáñez, M., Luo, Z., De Roo, J., Carrete, A., Dimitrievska, M., … Cabot, A. (2016). Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals. Chemistry of Materials, 28(3), 720–726. https://doi.org/10.1021/acs.chemmater.5b03417
Shavel, Alexey, Maria Ibáñez, Zhishan Luo, Jonathan De Roo, Alex Carrete, Mirjana Dimitrievska, Aziz Genç, et al. “Scalable Heating-up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals.” Chemistry of Materials 28, no. 3 (2016): 720–26. https://doi.org/10.1021/acs.chemmater.5b03417.
A. Shavel et al., “Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals,” Chemistry of Materials, vol. 28, no. 3, pp. 720–726, 2016.
Shavel A, Ibáñez M, Luo Z, De Roo J, Carrete A, Dimitrievska M, Genç A, Meyns M, Pérez Rodríguez A, Kovalenko M, Arbol J, Cabot A. 2016. Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals. Chemistry of Materials. 28(3), 720–726.
Shavel, Alexey, et al. “Scalable Heating-up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals.” Chemistry of Materials, vol. 28, no. 3, American Chemical Society, 2016, pp. 720–26, doi:10.1021/acs.chemmater.5b03417.

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